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Table of Contents
Intro
Preface
Contents
About the Editors
1 TKX-50: A Highly Promising Secondary Explosive
1 Introduction
2 Synthesis and Characterization of TKX-50
2.1 Synthesis and Improved Synthetic Routes
2.2 Spectroscopic Characterization
2.3 Solid-State Structure and Related Properties
3 Energetic Properties of TKX-50
3.1 IS, FS, and ESD
3.2 Heats of Formation, Combustion, and Explosion
3.3 Detonation Velocity and Pressure, Explosion Temperature, and Volume of Gaseous Detonation Products
3.4 Explosive Power and UNDEX
3.5 Thermal Stability and Aging
3.6 Compatibility
4 Nano-TKX-50
5 Formulations Containing TKX-50
5.1 PBXs Containing TKX-50
5.2 Melt-Cast Explosives Containing TKX-50
5.3 Composite Explosives Containing TKX-50
6 TKX-50 Cocrystals
7 Conclusions and Future Perspective
References
2 Stability Assessment for Double Base Rocket Propellant During Long Natural/Artificial Aging Using Various Methods and Kinetic Modeling
1 Introduction
2 Experimental and Methods
2.1 Materials
2.2 Artificial Aging
2.3 Density Measurement
2.4 FTIR Analysis
2.5 XRD Analysis
2.6 Stability Tests
2.7 Vacuum Stability Test
2.8 Kinetic Modeling on VST Data for the DBRP Thermal Decomposition
2.9 Storage Lifetime Prediction
3 Results and Discussion
3.1 Density Measurement
3.2 FTIR Analysis
3.3 XRD Analysis
3.4 Stability Tests
3.5 Kinetic Modeling
3.6 Storage Lifetime Prediction
4 Conclusion
References
3 Assessment of the Migration of Combustion Moderator in Nitrocellulose-Based Propellant
1 Introduction
2 Diffusion Models
3 Experimental Procedure
3.1 HPLC Measurement
3.2 Infrared Microscopy (IR) Measurement
4 Results
4.1 HPLC
4.2 IR Microscopy
5 Discussion
6 Conclusions
References
4 Study of the Chemical Stability of a Pseudo-Brookite B-Synroc by the MCC1, MCC2, and Microwaves Tests
1 Introduction
2 Experimental
3 Results and Discussions
4 Conclusion
References
5 Behavior Study of New Formulations Based on Plasticized Poly Vinyl Chloride Stabilized with Epoxidized Sunflower Oil
1 Introduction
2 Experimental
2.1 Products
2.2 Preparation of Formulations
2.3 Lixiviation Tests
2.4 In Situ Biodegradation of Polymer in Soil
3 Results and Discussion
3.1 Lixiviation Test
Preface
Contents
About the Editors
1 TKX-50: A Highly Promising Secondary Explosive
1 Introduction
2 Synthesis and Characterization of TKX-50
2.1 Synthesis and Improved Synthetic Routes
2.2 Spectroscopic Characterization
2.3 Solid-State Structure and Related Properties
3 Energetic Properties of TKX-50
3.1 IS, FS, and ESD
3.2 Heats of Formation, Combustion, and Explosion
3.3 Detonation Velocity and Pressure, Explosion Temperature, and Volume of Gaseous Detonation Products
3.4 Explosive Power and UNDEX
3.5 Thermal Stability and Aging
3.6 Compatibility
4 Nano-TKX-50
5 Formulations Containing TKX-50
5.1 PBXs Containing TKX-50
5.2 Melt-Cast Explosives Containing TKX-50
5.3 Composite Explosives Containing TKX-50
6 TKX-50 Cocrystals
7 Conclusions and Future Perspective
References
2 Stability Assessment for Double Base Rocket Propellant During Long Natural/Artificial Aging Using Various Methods and Kinetic Modeling
1 Introduction
2 Experimental and Methods
2.1 Materials
2.2 Artificial Aging
2.3 Density Measurement
2.4 FTIR Analysis
2.5 XRD Analysis
2.6 Stability Tests
2.7 Vacuum Stability Test
2.8 Kinetic Modeling on VST Data for the DBRP Thermal Decomposition
2.9 Storage Lifetime Prediction
3 Results and Discussion
3.1 Density Measurement
3.2 FTIR Analysis
3.3 XRD Analysis
3.4 Stability Tests
3.5 Kinetic Modeling
3.6 Storage Lifetime Prediction
4 Conclusion
References
3 Assessment of the Migration of Combustion Moderator in Nitrocellulose-Based Propellant
1 Introduction
2 Diffusion Models
3 Experimental Procedure
3.1 HPLC Measurement
3.2 Infrared Microscopy (IR) Measurement
4 Results
4.1 HPLC
4.2 IR Microscopy
5 Discussion
6 Conclusions
References
4 Study of the Chemical Stability of a Pseudo-Brookite B-Synroc by the MCC1, MCC2, and Microwaves Tests
1 Introduction
2 Experimental
3 Results and Discussions
4 Conclusion
References
5 Behavior Study of New Formulations Based on Plasticized Poly Vinyl Chloride Stabilized with Epoxidized Sunflower Oil
1 Introduction
2 Experimental
2.1 Products
2.2 Preparation of Formulations
2.3 Lixiviation Tests
2.4 In Situ Biodegradation of Polymer in Soil
3 Results and Discussion
3.1 Lixiviation Test