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Table of Contents
Intro
Foreword
Preface
Contents
1 Introduction to In-Situ Transmission Electron Microscopy
1.1 Definition of In-Situ Transmission Electron Microscopy
1.2 A Brief History of In-Situ Transmission Electron Microscopy
1.3 Modern In-Situ Transmission Electron Microscopy
1.4 Challenges and Opportunities
1.5 Concept of This Book
References
2 Electron Beam Irradiation Effects and In-Situ Irradiation of Nanomaterials
2.1 A Brief History of In-Situ Electron Irradiation
2.2 Fundamental Electron Irradiation Effects
2.2.1 Atom Displacements
2.2.2 Surface Sputtering
2.2.3 Electrostatic Charging
2.2.4 Radiolysis
2.2.5 Electron Beam Heating
2.2.6 Electron Beam-Induced Deposition
2.3 Electron Irradiation-Induced Processes in Nanomaterials
2.3.1 The Dynamics of Defects Under Electron Beam Irradiation
2.3.2 Irradiation-Induced Phase Transformations
2.3.3 Nucleation and Growth of Nanostructures Under Irradiation
2.3.4 Fabrication of New Structures Under Irradiation
2.3.5 Deformation of Nanostructures Under Electron Irradiation
2.4 Conclusions and Outlook
References
3 In-Situ Nanomechanical TEM
3.1 A Brief History of In Situ Nanomechanical TEM
3.2 Current In Situ TEM-based Mechanical Testing Techniques
3.2.1 Thin Film Straining Technique
3.2.2 TEM Grid Technique
3.2.3 Thermal-Bimetallic-Based Technique
3.2.4 MEMS-Based Techniques
3.2.5 Sequential Fabrication-Testing Technique
3.3 Typical Applications
3.3.1 Deformation of Metallic Nanowires
3.3.2 Deformation of Nanocrystalline Metals
3.3.3 Deformation at Grain Boundaries
3.3.4 Deformation Under Elevated Temperature
3.3.5 Deformation of "Brittle" Materials
3.4 Outlook
References
4 In-Situ Heating TEM
4.1 A Brief History of In-Situ Heating TEM
4.2 Current In-Situ Heating TEM Technologies
4.2.1 Operation Mode
4.2.2 Type of Heating Holders
4.2.3 Microheaters
4.2.4 Synergy with Heating
4.3 Research Based on In-Situ Heating TEM
4.3.1 Material Growth
4.3.2 Sublimation and Surface Energy
4.3.3 Failure Analysis
4.3.4 Annealing and Phase Transitions
4.3.5 Catalysis and Battery
4.3.6 Solid-State Amorphization and Crystallization
4.3.7 Degradation of Perovskite Solar Cells
4.4 Conclusions and Outlook
References
5 In-Situ Biasing TEM
5.1 Introduction
5.2 Electrical Measurements
5.2.1 Field Emission of Carbon Nanotubes and Nanowires
5.2.2 Quantum Conductance of Au Atomic Chain and MWCNT
5.2.3 Electrical and Mechanical Coupling
5.2.4 Ferroelectric Domain Switching
5.2.5 Resistive Switching
5.3 Electrothermal Behaviors and Measurements
5.3.1 Thermal Parameter Measurements
5.3.2 Joule Heating of Nanocarbon
5.4 In Situ TEM Nanoelectrochemistry
5.4.1 IL Cell
5.4.2 Solid Cell
5.4.3 In Situ Liquid Cell
5.5 Perspective
References
6 In-Situ Optical TEM
Foreword
Preface
Contents
1 Introduction to In-Situ Transmission Electron Microscopy
1.1 Definition of In-Situ Transmission Electron Microscopy
1.2 A Brief History of In-Situ Transmission Electron Microscopy
1.3 Modern In-Situ Transmission Electron Microscopy
1.4 Challenges and Opportunities
1.5 Concept of This Book
References
2 Electron Beam Irradiation Effects and In-Situ Irradiation of Nanomaterials
2.1 A Brief History of In-Situ Electron Irradiation
2.2 Fundamental Electron Irradiation Effects
2.2.1 Atom Displacements
2.2.2 Surface Sputtering
2.2.3 Electrostatic Charging
2.2.4 Radiolysis
2.2.5 Electron Beam Heating
2.2.6 Electron Beam-Induced Deposition
2.3 Electron Irradiation-Induced Processes in Nanomaterials
2.3.1 The Dynamics of Defects Under Electron Beam Irradiation
2.3.2 Irradiation-Induced Phase Transformations
2.3.3 Nucleation and Growth of Nanostructures Under Irradiation
2.3.4 Fabrication of New Structures Under Irradiation
2.3.5 Deformation of Nanostructures Under Electron Irradiation
2.4 Conclusions and Outlook
References
3 In-Situ Nanomechanical TEM
3.1 A Brief History of In Situ Nanomechanical TEM
3.2 Current In Situ TEM-based Mechanical Testing Techniques
3.2.1 Thin Film Straining Technique
3.2.2 TEM Grid Technique
3.2.3 Thermal-Bimetallic-Based Technique
3.2.4 MEMS-Based Techniques
3.2.5 Sequential Fabrication-Testing Technique
3.3 Typical Applications
3.3.1 Deformation of Metallic Nanowires
3.3.2 Deformation of Nanocrystalline Metals
3.3.3 Deformation at Grain Boundaries
3.3.4 Deformation Under Elevated Temperature
3.3.5 Deformation of "Brittle" Materials
3.4 Outlook
References
4 In-Situ Heating TEM
4.1 A Brief History of In-Situ Heating TEM
4.2 Current In-Situ Heating TEM Technologies
4.2.1 Operation Mode
4.2.2 Type of Heating Holders
4.2.3 Microheaters
4.2.4 Synergy with Heating
4.3 Research Based on In-Situ Heating TEM
4.3.1 Material Growth
4.3.2 Sublimation and Surface Energy
4.3.3 Failure Analysis
4.3.4 Annealing and Phase Transitions
4.3.5 Catalysis and Battery
4.3.6 Solid-State Amorphization and Crystallization
4.3.7 Degradation of Perovskite Solar Cells
4.4 Conclusions and Outlook
References
5 In-Situ Biasing TEM
5.1 Introduction
5.2 Electrical Measurements
5.2.1 Field Emission of Carbon Nanotubes and Nanowires
5.2.2 Quantum Conductance of Au Atomic Chain and MWCNT
5.2.3 Electrical and Mechanical Coupling
5.2.4 Ferroelectric Domain Switching
5.2.5 Resistive Switching
5.3 Electrothermal Behaviors and Measurements
5.3.1 Thermal Parameter Measurements
5.3.2 Joule Heating of Nanocarbon
5.4 In Situ TEM Nanoelectrochemistry
5.4.1 IL Cell
5.4.2 Solid Cell
5.4.3 In Situ Liquid Cell
5.5 Perspective
References
6 In-Situ Optical TEM