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Parts of this thesis have been published in the following journal articles:; Supervisor's Foreword; Acknowledgments; Contents; 1 Introduction; 1.1 Hydrogen Energy and Hydrogen Storage Materials; 1.1.1 The Signi cance of Hydrogen Energy; 1.1.2 Characteristics and Research Status of Hydrogen Energy; 1.1.3 Research Progress of Hydrogen Storage Materials; 1.1.4 Research Progress of Mg-Based Hydrogen Storage Materials; 1.1.4.1 Fabricating Particular Nanostructures; 1.1.4.2 Doping Catalysts; 1.1.4.3 Recombination with Porous Materials; 1.2 Hydrogen Storage Properties of Mg-Based Films
1.2.1 Preparation and Characterization of Mg-Based Films1.2.2 Research Progress of Mg-Based Hydrogen Storage Films; 1.3 Hydrogen-Induced Property Changes of Thin Films and the Applications; 1.4 Contents of This Thesis; References; 2 Experimental Methods; 2.1 Film Preparation; 2.2 Thin Film Characterization; 2.2.1 X-Ray Di raction; 2.2.2 Scanning Electron Microscope/Energy Dispersive Spectrum Analysis (SEM/EDS); 2.2.3 Transmission Electron Microscopy (TEM); 2.3 Property Measurements of Thin Films; 2.3.1 Electrical Resistance Measurements [1-3]; 2.3.2 Optical Transmittance Measurements [1-3]
2.3.3 Electrochemical Property Measurements [5, 6]References; 3 Structural Tailoring of Mg-Based Thin Films and Study of Their Hydrogen Storage Properties; 3.1 Introduction; 3.2 Experimental; 3.2.1 Film Preparation; 3.2.2 Structural Characterization and Property Measurements; 3.3 Results and Discussion; 3.3.1 Gaseous Hydrogen Storage Properties; 3.3.1.1 Structural Characterization; 3.3.1.2 Electrical and Optical Properties; 3.3.1.3 Hydrogen Sorption Kinetics; 3.3.2 Electrochemical Hydrogen Storage Properties; 3.3.3 Discussions; 3.4 Conclusions; References
4 Hydrogen Storage Properties of Mg-Based Thin Films with Di erent Interlayers4.1 Introduction; 4.2 Experimental; 4.2.1 Film Preparation; 4.2.2 Structural Characterization; 4.3 Results and Discussion; 4.3.1 Hydrogen Storage Properties of Mg-Ti-Pd Films; 4.3.1.1 Structural Characterization; 4.3.1.2 Electric Resistance Changes; 4.3.1.3 Optical Switching Properties; 4.3.1.4 Electrochemical Behaviors; 4.3.2 Hydrogen Storage Properties of Mg-Al-Pd Films; 4.3.2.1 Electric Resistance Changes; 4.3.2.2 Optical Switching Properties; 4.3.3 Mechanism and Discussion; 4.4 Conclusions; References
5 Gaseous and Electrochemical Hydrogen Storage Properties of Mg-Ti Multilayers5.1 Introduction; 5.2 Experimental; 5.2.1 Film Preparation; 5.2.2 Structural Characterization; 5.3 Results and Discussion; 5.3.1 Gaseous Hydrogen Storage Properties; 5.3.1.1 Structural Characterization; 5.3.1.2 Electric Resistance Changes; 5.3.1.3 Optical Switching Properties; 5.3.1.4 Gaseous Hydrogenation Mechanism; 5.3.2 Electrochemical Properties; 5.3.2.1 Electrochemical Charge-Discharge Properties; 5.3.2.2 Electrochemical Hydrogenation Mechanism; 5.4 Conclusions; References
1.2.1 Preparation and Characterization of Mg-Based Films1.2.2 Research Progress of Mg-Based Hydrogen Storage Films; 1.3 Hydrogen-Induced Property Changes of Thin Films and the Applications; 1.4 Contents of This Thesis; References; 2 Experimental Methods; 2.1 Film Preparation; 2.2 Thin Film Characterization; 2.2.1 X-Ray Di raction; 2.2.2 Scanning Electron Microscope/Energy Dispersive Spectrum Analysis (SEM/EDS); 2.2.3 Transmission Electron Microscopy (TEM); 2.3 Property Measurements of Thin Films; 2.3.1 Electrical Resistance Measurements [1-3]; 2.3.2 Optical Transmittance Measurements [1-3]
2.3.3 Electrochemical Property Measurements [5, 6]References; 3 Structural Tailoring of Mg-Based Thin Films and Study of Their Hydrogen Storage Properties; 3.1 Introduction; 3.2 Experimental; 3.2.1 Film Preparation; 3.2.2 Structural Characterization and Property Measurements; 3.3 Results and Discussion; 3.3.1 Gaseous Hydrogen Storage Properties; 3.3.1.1 Structural Characterization; 3.3.1.2 Electrical and Optical Properties; 3.3.1.3 Hydrogen Sorption Kinetics; 3.3.2 Electrochemical Hydrogen Storage Properties; 3.3.3 Discussions; 3.4 Conclusions; References
4 Hydrogen Storage Properties of Mg-Based Thin Films with Di erent Interlayers4.1 Introduction; 4.2 Experimental; 4.2.1 Film Preparation; 4.2.2 Structural Characterization; 4.3 Results and Discussion; 4.3.1 Hydrogen Storage Properties of Mg-Ti-Pd Films; 4.3.1.1 Structural Characterization; 4.3.1.2 Electric Resistance Changes; 4.3.1.3 Optical Switching Properties; 4.3.1.4 Electrochemical Behaviors; 4.3.2 Hydrogen Storage Properties of Mg-Al-Pd Films; 4.3.2.1 Electric Resistance Changes; 4.3.2.2 Optical Switching Properties; 4.3.3 Mechanism and Discussion; 4.4 Conclusions; References
5 Gaseous and Electrochemical Hydrogen Storage Properties of Mg-Ti Multilayers5.1 Introduction; 5.2 Experimental; 5.2.1 Film Preparation; 5.2.2 Structural Characterization; 5.3 Results and Discussion; 5.3.1 Gaseous Hydrogen Storage Properties; 5.3.1.1 Structural Characterization; 5.3.1.2 Electric Resistance Changes; 5.3.1.3 Optical Switching Properties; 5.3.1.4 Gaseous Hydrogenation Mechanism; 5.3.2 Electrochemical Properties; 5.3.2.1 Electrochemical Charge-Discharge Properties; 5.3.2.2 Electrochemical Hydrogenation Mechanism; 5.4 Conclusions; References