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000756196 019__ $$a952571191
000756196 020__ $$a9783319313290$$q(electronic book)
000756196 020__ $$a3319313290$$q(electronic book)
000756196 020__ $$z9783319313276
000756196 0247_ $$a10.1007/978-3-319-31329-0$$2doi
000756196 035__ $$aSP(OCoLC)ocn952934113
000756196 035__ $$aSP(OCoLC)952934113$$z(OCoLC)952571191
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000756196 050_4 $$aQC291
000756196 050_4 $$aTA401-492
000756196 08204 $$a536/.6$$223
000756196 08204 $$a620.11
000756196 24500 $$aFast scanning calorimetry$$h[electronic resource] /$$cChristoph Schick, Vincent Mathot, editors.
000756196 260__ $$aCham :$$bSpringer,$$c2016.
000756196 300__ $$a1 online resource (796 pages)
000756196 336__ $$atext$$btxt$$2rdacontent
000756196 337__ $$acomputer$$bc$$2rdamedia
000756196 338__ $$aonline resource$$bcr$$2rdacarrier
000756196 500__ $$a1.4.5.3 Cooling Rate Dependence of the Glass Transition
000756196 500__ $$aIncludes index.
000756196 5050_ $$aPreface; Contents; About the Editors; Part I: Advanced Instrumentation, Techniques and Methods; Chapter 1: Material Characterization by Fast Scanning Calorimetry: Practice and Applications; 1.1 Introduction; 1.2 Instrumental; 1.2.1 General Aspects; 1.2.1.1 The Calorimeter; 1.2.1.2 The Sample; 1.2.2 Design of the Flash DSC; 1.2.3 The Flash DSC Sensor; 1.2.3.1 Sensor Design; 1.2.3.2 Operation Mode; 1.2.3.3 Placing a Chip-Sensor into the Flash DSC; 1.2.4 Properties of the Flash DSC; 1.2.4.1 Possible Scanning Rates and Purge Gas; 1.2.4.2 Thermal Lag; 1.2.4.3 Isothermal Behavior
000756196 5058_ $$a1.2.4.4 Temperature Correction1.2.4.5 Dynamic Temperature Gradients; 1.2.4.6 Static Temperature Gradients; 1.2.4.7 Relation Between Scanning Rates and Sample Size; 1.2.5 Comments Regarding the Temperature Program; 1.2.6 Blank Correction; 1.2.6.1 The Blank Correction in Conventional DSC; 1.2.6.2 The Blank Correction in the Flash DSC; 1.2.6.3 Influence of Mechanical Interaction Between Sample and Sensor on the Measured Curve; 1.2.6.4 Reduction of the Mechanical Interaction; 1.3 Sample Preparation; 1.3.1 General Comments; 1.3.2 Polymers; 1.3.3 Low Molecular Organic Materials
000756196 5058_ $$a1.3.4 Metallic Glasses1.3.5 Estimation of the Sample Size; 1.3.5.1 Sample Size Estimation for Metallic Glass Alloys; 1.3.5.2 Sample Size Estimation for Polymers; Analyses of the Melting Peak; Analyses of the Glass Transition; Analyses of the Heat Capacity; Analyses of the Volume; 1.3.6 Determination of Sample Size Depending Effects (Critical Sample Size); 1.3.7 Measurements of the Initial Sample at the First Heating Run; 1.3.8 General Comments About the Use of Oil as a Contact Medium; 1.3.8.1 Selection and Behavior of Oil; 1.3.8.2 Application of an Oil Film
000756196 5058_ $$a1.3.8.3 Limitation of the Use of Silicone Oil as Contact Medium1.4 Concepts of Polymer Analysis; 1.4.1 Polymers Are Meta Stable Materials; 1.4.2 Measurement of Crystallization Effects; 1.4.2.1 General Comments; 1.4.2.2 Typical Temperature Programs; 1.4.2.3 Example: Influence of Nucleating Agents and Additives on the Crystallization of Poly(Butadiene Terephthalate) Polymers; 1.4.2.4 Example: Cold Crystallization of Isotactic Polypropylene; 1.4.3 Analyses of Melting Processes; 1.4.3.1 Reorganization During Heating; 1.4.3.2 Example: Reorganization of Isotactic Polypropylene
000756196 5058_ $$a1.4.3.3 Influence of the Heating Rate on the Temperature of Melting PeaksMelting of Stable Crystals Without Superheating; Melting of Stable Crystals with Superheating; 1.4.3.4 Example: Melting of Isotactic Polypropylene; 1.4.3.5 Example: Melting of Poly(Ethylene Terephthalate); 1.4.4 Investigation of Polymer Stability; 1.4.4.1 General Comments and Typical Temperature Programs; 1.4.4.2 Example: Stability of Poly(Etheretherketone); 1.4.5 Analysis of the Noncrystalline Fractions; 1.4.5.1 The Three-Phase Model; 1.4.5.2 Determination of the Amorphous Phases
000756196 506__ $$aAccess limited to authorized users.
000756196 520__ $$aIn the past decades, the scan rate range of calorimeters has been extended tremendously at the high end, from approximately 10 up to 10 000 000 °C/s and more. The combination of various calorimeters and the newly-developed Fast Scanning Calorimeters (FSC) now span 11 orders of magnitude, by which many processes can be mimicked according to the time scale(s) of chemical and physical transitions occurring during cooling, heating and isothermal stays in case heat is exchanged. This not only opens new areas of research on polymers, metals, pharmaceuticals and all kinds of substances with respect to glass transition, crystallization and melting phenomena, it also enables in-depth study of metastability and reorganization of samples on an 1 to 1000 ng scale. In addition, FSC will become a crucial tool for understanding and optimization of processing methods at high speeds like injection molding. The book resembles the state-of-the art in Thermal Analysis & Calorimetry and is an excellent starting point for both experts and newcomers in the field.
000756196 588__ $$aDescription based on print version record.
000756196 650_0 $$aCalorimetry.
000756196 650_0 $$aMaterials science.
000756196 650_0 $$aPolymers.
000756196 650_0 $$aChemical engineering.
000756196 650_0 $$aThermodynamics.
000756196 650_0 $$aHeat engineering.
000756196 650_0 $$aHeat$$xTransmission.
000756196 650_0 $$aMass transfer.
000756196 7001_ $$aSchick, Christoph.
000756196 7001_ $$aMathot, Vincent.
000756196 77608 $$iPrint version:$$aSchick, Christoph$$tFast Scanning Calorimetry$$dCham : Springer International Publishing,c2016$$z9783319313276
000756196 852__ $$bebk
000756196 85640 $$3SpringerLink$$uhttps://univsouthin.idm.oclc.org/login?url=http://link.springer.com/10.1007/978-3-319-31329-0$$zOnline Access$$91397441.1
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000756196 980__ $$aEBOOK
000756196 980__ $$aBIB
000756196 982__ $$aEbook
000756196 983__ $$aOnline
000756196 994__ $$a92$$bISE