Nanoscale AFM and TEM observations of elementary dislocation mechanisms / Jozef Veselý.
2017
TN690
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Title
Nanoscale AFM and TEM observations of elementary dislocation mechanisms / Jozef Veselý.
Author
ISBN
9783319483023 (electronic book)
3319483021 (electronic book)
9783319483016
3319483013
3319483021 (electronic book)
9783319483016
3319483013
Publication Details
Cham, Switzerland : Springer, 2017.
Language
English
Description
1 online resource.
Item Number
10.1007/978-3-319-48302-3 doi
Call Number
TN690
Dewey Decimal Classification
669/.96141
Summary
This thesis addresses elementary dislocation processes occurring in single-crystalline alloys based on Fe-Al, and investigates correspondences between dislocation distribution inside crystals characterized by transmission electron microscopy (TEM) and surface patterns observed using atomic force microscopy (AFM). Fe-Al alloys with different degrees of ordering were prepared and deformed in compression at ambient temperature in-situ inside the AFM device. The evolution of slip line structures was captured in the sequences of AFM images and wavy slip bands, while cross slip at the tip of the slip band and homogeneous fine slip lines were also identified. Further, the thesis develops a technique for constructing 3D representations of dislocations observed by TEM without the prohibitive difficulties of tomography, and creates 3D models of dislocation structures. Generally speaking, the thesis finds good agreement between AFM and TEM observations, confirming the value of AFM as a relevant tool for studying dislocations.
Note
"Doctoral thesis accepted by Charles University, Prague, Czech Republic."
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text file PDF
Series
Springer theses.
Available in Other Form
Print version: 9783319483016
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Table of Contents
Introduction
Iron-Rich Iron Aluminides
Experimental Methods
Results
Discussion
Summary.
Iron-Rich Iron Aluminides
Experimental Methods
Results
Discussion
Summary.