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Intro; Supervisor's Foreword; Abstract; Parts of this thesis have been published as the following journal articles:; Contents; 1 Introduction; 1.1 Metal-Organic Framework Nanomaterials; 1.1.1 Brief Introduction of Metal-Organic Frameworks; 1.1.2 The Characters of Metal-Organic Frameworks; 1.1.3 The Synthesis of Metal-Organic Frameworks; 1.1.4 Applications of Metal-Organic Frameworks; 1.2 Metal-Organic Framework Derived Nanomaterials; 1.2.1 Metal-Organic Framework Derived Porous Carbons; 1.2.2 Metal-Organic Framework Derived Metal Oxides.
1.2.3 Metal-Organic Framework Derived Metal Oxide/Carbon Composites1.2.4 Other Metal-Organic Framework Derived Inorganic Compounds; 1.3 The Application of MOF-Derived Materials in Electrochemical Energy Storage and Conversion; 1.3.1 MOF-Derived Materials for Supercapacitor; 1.3.2 MOF-Derived Materials for Lithium-Ion Batteries; 1.3.3 MOF-Derived Materials for Fuel Cells; 1.3.4 Applications in Other Electrochemical Processes; 1.4 The Significance of This Study and Research Content; References; 2 Synthesis and Characterization of MOF-Derived Nanomaterials; 2.1 Instruments and Chemicals.
2.1.1 Instruments2.1.2 Chemicals Used in Synthesis of N-Doped Nanoparticles; 2.1.3 Chemicals Used in Synthesis of Core-Shell Metal Oxide Nanoparticles; 2.1.4 Chemicals Used in Synthesis of Hollow Metal Oxide Nanoparticles; 2.1.5 Chemicals Used in Synthesis of 3D Porous Carbon; 2.2 Synthesis of N-Doped Carbon Nanoparticles; 2.2.1 Synthesis of Co-MOF with Different Sizes; 2.2.2 Synthesis of Multi-component ZnCo-MOF; 2.2.3 Synthesis of N-Doped Carbon Nanomaterials; 2.3 Synthesis of Core-Shell Metal Oxide Nanoparticles; 2.3.1 Synthesis of Ordered Porous Carbon Matrix; 2.3.2 Zif-9@CM.
2.3.3 Synthesis of Core-Shell Metal Oxide Nanoparticles2.4 Synthesis of Hollow Metal Oxide Nanoparticles; 2.4.1 Synthesis of Nitrogen-Doped Graphene Aerogel; 2.4.2 Nitrogen-Doped Graphene Aerogel Supported Co-MOF; 2.4.3 Synthesis of Hollow Metal Oxide Nanoparticles; 2.5 Synthesis of 3D Porous Carbon; 2.5.1 Synthesis of Metal-Organic Aerogel/Xerogel; 2.5.2 Synthesis of 3D Porous Carbon from MOA; 2.5.3 Synthesis of Porous Carbon from MOX; 2.6 Characterization of Materials; 2.6.1 X-Ray Diffraction (XRD); 2.6.2 Thermogravimetric Analysis (TGA); 2.6.3 Energy Dispersive Spectroscopy (EDS).
2.6.4 X-Ray Photoelectron Spectroscopy (XPS)2.6.5 Inductively Coupled Plasma (ICP); 2.6.6 Raman Spectroscopy; 2.6.7 Nitrogen Sorption Measurement; 2.6.8 Scanning Electron Microscope (SEM); 2.6.9 Transmission Electron Microscope (TEM); 2.7 Electrochemical Measurements; 2.7.1 ORR Measurements; 2.7.2 Battery Test; References; 3 Formation of N-Doped Carbon Nanomaterials for ORR Catalysis and Li Storage; 3.1 Introduction; 3.2 Synthesis of N-Doped Carbon Nanoparticles; 3.2.1 Formation of Co-MOFs of Different Particle Sizes; 3.2.2 Formation of Multi-component ZnCo-MOF.
1.2.3 Metal-Organic Framework Derived Metal Oxide/Carbon Composites1.2.4 Other Metal-Organic Framework Derived Inorganic Compounds; 1.3 The Application of MOF-Derived Materials in Electrochemical Energy Storage and Conversion; 1.3.1 MOF-Derived Materials for Supercapacitor; 1.3.2 MOF-Derived Materials for Lithium-Ion Batteries; 1.3.3 MOF-Derived Materials for Fuel Cells; 1.3.4 Applications in Other Electrochemical Processes; 1.4 The Significance of This Study and Research Content; References; 2 Synthesis and Characterization of MOF-Derived Nanomaterials; 2.1 Instruments and Chemicals.
2.1.1 Instruments2.1.2 Chemicals Used in Synthesis of N-Doped Nanoparticles; 2.1.3 Chemicals Used in Synthesis of Core-Shell Metal Oxide Nanoparticles; 2.1.4 Chemicals Used in Synthesis of Hollow Metal Oxide Nanoparticles; 2.1.5 Chemicals Used in Synthesis of 3D Porous Carbon; 2.2 Synthesis of N-Doped Carbon Nanoparticles; 2.2.1 Synthesis of Co-MOF with Different Sizes; 2.2.2 Synthesis of Multi-component ZnCo-MOF; 2.2.3 Synthesis of N-Doped Carbon Nanomaterials; 2.3 Synthesis of Core-Shell Metal Oxide Nanoparticles; 2.3.1 Synthesis of Ordered Porous Carbon Matrix; 2.3.2 Zif-9@CM.
2.3.3 Synthesis of Core-Shell Metal Oxide Nanoparticles2.4 Synthesis of Hollow Metal Oxide Nanoparticles; 2.4.1 Synthesis of Nitrogen-Doped Graphene Aerogel; 2.4.2 Nitrogen-Doped Graphene Aerogel Supported Co-MOF; 2.4.3 Synthesis of Hollow Metal Oxide Nanoparticles; 2.5 Synthesis of 3D Porous Carbon; 2.5.1 Synthesis of Metal-Organic Aerogel/Xerogel; 2.5.2 Synthesis of 3D Porous Carbon from MOA; 2.5.3 Synthesis of Porous Carbon from MOX; 2.6 Characterization of Materials; 2.6.1 X-Ray Diffraction (XRD); 2.6.2 Thermogravimetric Analysis (TGA); 2.6.3 Energy Dispersive Spectroscopy (EDS).
2.6.4 X-Ray Photoelectron Spectroscopy (XPS)2.6.5 Inductively Coupled Plasma (ICP); 2.6.6 Raman Spectroscopy; 2.6.7 Nitrogen Sorption Measurement; 2.6.8 Scanning Electron Microscope (SEM); 2.6.9 Transmission Electron Microscope (TEM); 2.7 Electrochemical Measurements; 2.7.1 ORR Measurements; 2.7.2 Battery Test; References; 3 Formation of N-Doped Carbon Nanomaterials for ORR Catalysis and Li Storage; 3.1 Introduction; 3.2 Synthesis of N-Doped Carbon Nanoparticles; 3.2.1 Formation of Co-MOFs of Different Particle Sizes; 3.2.2 Formation of Multi-component ZnCo-MOF.