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Intro; Foreword; Contents; Chapter 1: Mechanism of Photocatalysis; 1.1 Introduction; 1.2 TiO2 Photocatalysis; 1.3 Mechanism of Photocatalytic Oxidation Reactions; 1.4 Influence of Different Parameters on the Degradation of Pollutants; 1.4.1 Catalyst Loading; 1.4.2 pH Effect; 1.4.3 Surface Area and Morphology; 1.4.4 Effect of Temperature; 1.4.5 Effect of Contaminant Concentration; 1.4.6 Influence of Calcination Temperature; References; Chapter 2: In Situ Characterization of Photocatalytic Activity; 2.1 Fluorescence; 2.1.1 Types of Probing Agents for ROS; 2.1.2 Single-Molecule Spectroscopy
2.2 Infrared Spectroscopy2.2.1 Gas-Phase Photocatalysis; 2.2.2 Aqueous-Phase Photocatalysis; 2.3 Raman; 2.4 In Situ Atomic Force Microscopy and Fluorescence; 2.5 In Situ NMR and ESR; References; Chapter 3: Titanium-Based Mesoporous Materials for Photocatalysis; 3.1 The History of Mesoporous Materials; 3.2 The Development of Mesoporous TiO2 in Photocatalysis; 3.2.1 The Preparation of Mesoporous TiO2; 3.2.2 Doping Modification on Mesoporous TiO2; 3.2.3 Mesoporous TiO2-Graphene Materials; 3.3 The Development of TiO2-SiO2 Mesoporous Materials
3.3.1 The Preparation of TiO2-SiO2 Mesoporous Materials3.3.2 The Application of TiO2-SiO2 Mesoporous Materials in Photocatalysis; 3.3.2.1 Photodegradation of Organic Pollutants; 3.3.2.2 Water Splitting; 3.4 Visible Light Response Metal-Organic Frameworks (MOFs); 3.5 The Development of Mesoporous Ti-SiO2 Materials in Photocatalysis; 3.5.1 The Preparation of Ti-SiO2 Mesoporous Materials; 3.5.2 The Application of Ti-SiO2 Mesoporous Materials in Photocatalysis; 3.5.2.1 CO2 Photoreduction; 3.5.2.2 NO/NO2 Photoreduction; 3.6 Conclusion; References
Chapter 4: Preparation of Reduced TiO2-x for Photocatalysis4.1 Introduction; 4.2 Synthesis of TiO2-x Photocatalysts; 4.2.1 Reduction Method; 4.2.1.1 Thermal Treatment Under Reducing Gases; 4.2.1.2 Vacuum Activation Treatment; 4.2.1.3 Metal Reduction; 4.2.1.4 Plasma Reduction; 4.2.1.5 Electrochemical Reduction; 4.2.1.6 UV Light Irradiation Reduction; 4.2.2 Oxidation Method; 4.2.2.1 Starting from Metallic Ti Powder; 4.2.2.2 Starting Form Ti(II) Precursors; 4.2.2.3 Starting from Ti(III) Precursors; 4.3 Properties of TiO2-x Photocatalysts; 4.4 Applications of TiO2-x Photocatalysts
4.5 Modification on TiO2-x Photocatalysts4.5.1 TiO2-x Doped with Nonmetal Elements; 4.5.2 TiO2-x Grafted with Metals; 4.5.3 TiO2-x Composited with Carbon; 4.5.4 TiO2-x Composited with Other Compounds; 4.5.5 TiO2-x with Ordered Morphology; 4.5.6 TiO2-x with Special Facets Exposed; 4.6 Summary and Outlook; References; Chapter 5: Graphene-Modified TiO2 with Enhanced Visible Light Photocatalytic Activities; 5.1 Introduction; 5.2 TiO2/Graphene Composite; 5.2.1 Two-Dimensional TiO2/Graphene Composites; 5.2.1.1 Preparations; 5.2.1.2 Characterizations; 5.2.2 Three-Dimensional TiO2/Graphene Composite
2.2 Infrared Spectroscopy2.2.1 Gas-Phase Photocatalysis; 2.2.2 Aqueous-Phase Photocatalysis; 2.3 Raman; 2.4 In Situ Atomic Force Microscopy and Fluorescence; 2.5 In Situ NMR and ESR; References; Chapter 3: Titanium-Based Mesoporous Materials for Photocatalysis; 3.1 The History of Mesoporous Materials; 3.2 The Development of Mesoporous TiO2 in Photocatalysis; 3.2.1 The Preparation of Mesoporous TiO2; 3.2.2 Doping Modification on Mesoporous TiO2; 3.2.3 Mesoporous TiO2-Graphene Materials; 3.3 The Development of TiO2-SiO2 Mesoporous Materials
3.3.1 The Preparation of TiO2-SiO2 Mesoporous Materials3.3.2 The Application of TiO2-SiO2 Mesoporous Materials in Photocatalysis; 3.3.2.1 Photodegradation of Organic Pollutants; 3.3.2.2 Water Splitting; 3.4 Visible Light Response Metal-Organic Frameworks (MOFs); 3.5 The Development of Mesoporous Ti-SiO2 Materials in Photocatalysis; 3.5.1 The Preparation of Ti-SiO2 Mesoporous Materials; 3.5.2 The Application of Ti-SiO2 Mesoporous Materials in Photocatalysis; 3.5.2.1 CO2 Photoreduction; 3.5.2.2 NO/NO2 Photoreduction; 3.6 Conclusion; References
Chapter 4: Preparation of Reduced TiO2-x for Photocatalysis4.1 Introduction; 4.2 Synthesis of TiO2-x Photocatalysts; 4.2.1 Reduction Method; 4.2.1.1 Thermal Treatment Under Reducing Gases; 4.2.1.2 Vacuum Activation Treatment; 4.2.1.3 Metal Reduction; 4.2.1.4 Plasma Reduction; 4.2.1.5 Electrochemical Reduction; 4.2.1.6 UV Light Irradiation Reduction; 4.2.2 Oxidation Method; 4.2.2.1 Starting from Metallic Ti Powder; 4.2.2.2 Starting Form Ti(II) Precursors; 4.2.2.3 Starting from Ti(III) Precursors; 4.3 Properties of TiO2-x Photocatalysts; 4.4 Applications of TiO2-x Photocatalysts
4.5 Modification on TiO2-x Photocatalysts4.5.1 TiO2-x Doped with Nonmetal Elements; 4.5.2 TiO2-x Grafted with Metals; 4.5.3 TiO2-x Composited with Carbon; 4.5.4 TiO2-x Composited with Other Compounds; 4.5.5 TiO2-x with Ordered Morphology; 4.5.6 TiO2-x with Special Facets Exposed; 4.6 Summary and Outlook; References; Chapter 5: Graphene-Modified TiO2 with Enhanced Visible Light Photocatalytic Activities; 5.1 Introduction; 5.2 TiO2/Graphene Composite; 5.2.1 Two-Dimensional TiO2/Graphene Composites; 5.2.1.1 Preparations; 5.2.1.2 Characterizations; 5.2.2 Three-Dimensional TiO2/Graphene Composite