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Table of Contents
Chapter 1
Carbon-based CO2 Adsorbents; 1.1 Introduction; 1.2 Porous Carbons; 1.2.1 Chemical Activation; 1.2.1.1 KOH as an Activating Agent; 1.2.1.2 Other Chemicals as Activating Agents; 1.2.2 Physical Activation; 1.2.2.1 CO2 as an Activating Agent; 1.2.2.2 Steam as an Activating Agent; 1.2.3 Metal Ion Activation; 1.2.4 Templating Method; 1.2.4.1 Porous Silica as a Hard Template; 1.2.4.2 Zeolite as a Hard Template; 1.2.4.3 Porous Organic Frameworks as Self-templates; 1.2.4.4 Carbide Lattices as Self-templates.
1.2.4.5 Triblock Copolymer as a Soft Template1.2.5 Combined Method of Templating and Activation; 1.2.5.1 Two-step Process; 1.2.5.2 One-step Process; 1.3 Graphene-based Porous Materials; 1.3.1 Graphene-based Adsorbents by Chemical Activation; 1.3.2 Graphene-based Adsorbents by Physical Activation; 1.3.3 Graphene-based Adsorbents by Other Techniques; 1.4 Carbon Nanotubes; 1.5 Carbon-based Hybrid Adsorbents; 1.5.1 Carbon-Organic Hybrid Adsorbents; 1.5.2 Carbon-Inorganic Hybrid Adsorbents; 1.6 Effect of Carbon Structure on CO2 Adsorption; 1.6.1 Pore Size Effect; 1.6.1.1 Analysis of Porosity.
1.6.1.2 Micropore Filling Mechanism of CO2 Adsorption1.6.1.3 Pore Size Effect at Different Sorption Pressures; 1.6.1.4 Pore Size Effect at Different Adsorption Temperatures; 1.6.2 Surface Chemistry Effect on CO2 Adsorption; 1.6.2.1 Effect of Nitrogen Doping; 1.6.2.2 Effect of Other Heteroatom-doping; 1.7 Summary and Outlook; Acknowledgements; References; Chapter 2
Zeolite and Silica-based CO2 Adsorbents; 2.1 Introduction; 2.2 (Alkali) Silicates; 2.2.1 Silicate Amine-based Adsorbents; 2.2.1.1 CO2 Absorption in Aqueous Alkanolamine Solutions; 2.2.2 Synthesis of Amine-Silica Adsorbents.
2.2.2.1 Impregnation Method2.2.2.2 Post-synthesis Grafting; 2.2.2.3 Direct Condensation; 2.2.3 CO2 Capture by Amine-Silica-based Adsorbents; 2.2.3.1 Amine Impregnated on Silica; 2.2.3.1.1 Effect of Temperature. As demonstrated by Xu et al.,48,54 a decrease in temperature from 75 °C to 25 °C causes a dramatic decreas ... ; 2.2.3.1.2 Effect of CO2 Partial Pressure. CO2 adsorption capacity is also influenced by the partial pressure of CO2 in the gas feed. Regard ...
2.2.3.1.3 Effect of Water. Xu et al. also studied the influence of water on CO2 adsorption capacity using PEI (50 wt%)/MCM-41. The authors ... 2.2.3.1.4 Effect of Percentage of Impregnation. According to the work of Xu et al.,48 the amount of amine (PEI) deposited on MCM-41 mesopor ... ; 2.2.3.1.5 Effect of the Support Structure. There is also a correlation between the CO2 adsorption capacities of amines impregnated on diffe ... ; 2.2.3.1.6 Effect of the Mesopores Structuring Agent. CO2 capture was tested with tetraethylenepentamine (TEPA) impregnated on MCM-41 and SB ...
Carbon-based CO2 Adsorbents; 1.1 Introduction; 1.2 Porous Carbons; 1.2.1 Chemical Activation; 1.2.1.1 KOH as an Activating Agent; 1.2.1.2 Other Chemicals as Activating Agents; 1.2.2 Physical Activation; 1.2.2.1 CO2 as an Activating Agent; 1.2.2.2 Steam as an Activating Agent; 1.2.3 Metal Ion Activation; 1.2.4 Templating Method; 1.2.4.1 Porous Silica as a Hard Template; 1.2.4.2 Zeolite as a Hard Template; 1.2.4.3 Porous Organic Frameworks as Self-templates; 1.2.4.4 Carbide Lattices as Self-templates.
1.2.4.5 Triblock Copolymer as a Soft Template1.2.5 Combined Method of Templating and Activation; 1.2.5.1 Two-step Process; 1.2.5.2 One-step Process; 1.3 Graphene-based Porous Materials; 1.3.1 Graphene-based Adsorbents by Chemical Activation; 1.3.2 Graphene-based Adsorbents by Physical Activation; 1.3.3 Graphene-based Adsorbents by Other Techniques; 1.4 Carbon Nanotubes; 1.5 Carbon-based Hybrid Adsorbents; 1.5.1 Carbon-Organic Hybrid Adsorbents; 1.5.2 Carbon-Inorganic Hybrid Adsorbents; 1.6 Effect of Carbon Structure on CO2 Adsorption; 1.6.1 Pore Size Effect; 1.6.1.1 Analysis of Porosity.
1.6.1.2 Micropore Filling Mechanism of CO2 Adsorption1.6.1.3 Pore Size Effect at Different Sorption Pressures; 1.6.1.4 Pore Size Effect at Different Adsorption Temperatures; 1.6.2 Surface Chemistry Effect on CO2 Adsorption; 1.6.2.1 Effect of Nitrogen Doping; 1.6.2.2 Effect of Other Heteroatom-doping; 1.7 Summary and Outlook; Acknowledgements; References; Chapter 2
Zeolite and Silica-based CO2 Adsorbents; 2.1 Introduction; 2.2 (Alkali) Silicates; 2.2.1 Silicate Amine-based Adsorbents; 2.2.1.1 CO2 Absorption in Aqueous Alkanolamine Solutions; 2.2.2 Synthesis of Amine-Silica Adsorbents.
2.2.2.1 Impregnation Method2.2.2.2 Post-synthesis Grafting; 2.2.2.3 Direct Condensation; 2.2.3 CO2 Capture by Amine-Silica-based Adsorbents; 2.2.3.1 Amine Impregnated on Silica; 2.2.3.1.1 Effect of Temperature. As demonstrated by Xu et al.,48,54 a decrease in temperature from 75 °C to 25 °C causes a dramatic decreas ... ; 2.2.3.1.2 Effect of CO2 Partial Pressure. CO2 adsorption capacity is also influenced by the partial pressure of CO2 in the gas feed. Regard ...
2.2.3.1.3 Effect of Water. Xu et al. also studied the influence of water on CO2 adsorption capacity using PEI (50 wt%)/MCM-41. The authors ... 2.2.3.1.4 Effect of Percentage of Impregnation. According to the work of Xu et al.,48 the amount of amine (PEI) deposited on MCM-41 mesopor ... ; 2.2.3.1.5 Effect of the Support Structure. There is also a correlation between the CO2 adsorption capacities of amines impregnated on diffe ... ; 2.2.3.1.6 Effect of the Mesopores Structuring Agent. CO2 capture was tested with tetraethylenepentamine (TEPA) impregnated on MCM-41 and SB ...