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000890310 019__ $$a1101374558
000890310 020__ $$a9783658263249$$q(electronic book)
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000890310 0247_ $$a10.1007/978-3-658-26324-9$$2doi
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000890310 035__ $$aSP(OCoLC)1100767823$$z(OCoLC)1101374558
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000890310 08204 $$a546/.22$$223
000890310 1001_ $$aTonauer, Christina Maria,$$eauthor.
000890310 24510 $$aGlassy nuclei in amorphous ice :$$bnovel evidence for the two-liquids nature of water /$$cChristina Maria Tonauer.
000890310 264_1 $$aWiesbaden :$$bSpringer Spektrum,$$c2019.
000890310 300__ $$a1 online resource (xiii, 76 pages) :$$billustrations.
000890310 336__ $$atext$$btxt$$2rdacontent
000890310 337__ $$acomputer$$bc$$2rdamedia
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000890310 4901_ $$aBestMasters,$$x2625-3577
000890310 5050_ $$aIntro; Dank; Contents; List of Figures; List of Tables; 1 Introduction; 1.1 Water, a truly anomalous substance; 1.2 State diagram of water; 1.2.1 Crystalline Phases; 1.2.1.1 Ice I: Hexagonal ice Ih, cubic ice Ic and stacking-disordered ice Isd; 1.2.1.2 Ices II, V, IX; 1.2.2 Amorphous states of ice; 1.2.2.1 Low-density amorphous ice (LDA); 1.2.2.2 High-density amorphous ice (HDA); 1.2.2.3 Very high-density amorphous ice (VHDA); 1.3 Phase transitions; 1.3.1 Classification [122-124]; 1.3.2 Homogeneous nucleation [125, 126] and nuclei growth; 1.3.3 Discontinuous transition between LDA/HDA
000890310 5058_ $$a1.4 Glass transition [125, 138, 139]1.4.1 Glass transitions in water; 1.5 Theories aimed at explaining water's anomalies [47, 48]; 1.6 Experimental challenges -- Water's no-man's land; 1.7 Motivation for the present thesis; 2 Methods; 2.1 Dilatometry [166]; 2.1.1 Dilatometric setup [166, 167]; 2.1.2 Sample preparation [167]; 2.2.1 X-ray diffraction setup; 3 Experimental section [167]; 3.1 Preparation of eHDA; 3.1.1 Isothermal compression of hexagonal ice Ih → uHDA; 3.1.2 Preparation of VHDA via isobaric heating of uHDA; 3.1.3 Preparation of eHDA via isothermal decompression of VHDA
000890310 5058_ $$a3.2 Crystallisation experiments of eHDA3.2.1 Crystallisation of eHDA (first isobaric heating step); 3.2.2 Second isobaric heating step to Tmax and quench recovery; 3.3 Definition of crystallisation temperature Tx; 3.4 Apparatus correction; 3.5 Temperature correction; 3.6 Characterisation of crystallisation products; 3.7 Results of the volumetric crystallisation study of eHDA; 3.8 Results of XRD study of crystallisation products of eHDA; 3.9 Crystallisation / polymorphic transition studies of bulk LDA / Ih; 3.9.1 Preparation of bulk LDA and Ih samples
000890310 5058_ $$a3.9.2 Isobaric heating experiments of bulk LDA/ice Ih and XRD characterisation4 Discussion [167]; 4.1 Crystallisation of eHDA; 4.2 Comparison of phase transition in the bulk and in nanosized nuclei; 5 Summary [166]; References
000890310 506__ $$aAccess limited to authorized users.
000890310 588__ $$aTitle details screen.
000890310 650_0 $$aWater.
000890310 650_0 $$aAmorphous substances.
000890310 77608 $$iPrint version $$z3658263237$$z9783658263232$$w(OCoLC)1091845130
000890310 830_0 $$aBestMasters.
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000890310 85640 $$3SpringerLink$$uhttps://univsouthin.idm.oclc.org/login?url=http://link.springer.com/10.1007/978-3-658-26324-9$$zOnline Access$$91397441.1
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