000890368 000__ 05189cam\a2200553Ii\4500 000890368 001__ 890368 000890368 005__ 20230306150058.0 000890368 006__ m\\\\\o\\d\\\\\\\\ 000890368 007__ cr\cn\nnnunnun 000890368 008__ 190513s2019\\\\si\\\\\\ob\\\\001\0\eng\d 000890368 019__ $$a1105196915 000890368 020__ $$a9789811369674$$q(electronic book) 000890368 020__ $$a9811369674$$q(electronic book) 000890368 020__ $$z9789811369650 000890368 0247_ $$a10.1007/978-981-13-6 000890368 035__ $$aSP(OCoLC)on1101101086 000890368 035__ $$aSP(OCoLC)1101101086$$z(OCoLC)1105196915 000890368 040__ $$aN$T$$beng$$erda$$epn$$cN$T$$dN$T$$dEBLCP$$dGW5XE$$dUKMGB$$dOCLCF$$dLQU 000890368 049__ $$aISEA 000890368 050_4 $$aHD9585.Z462 000890368 08204 $$a338.7666025$$223 000890368 1001_ $$aXu, Jun,$$eauthor. 000890368 24510 $$aSolid-State NMR in zeolite catalysis /$$cJun Xu, Qiang Wang, Shenhui Li and Feng Deng. 000890368 264_1 $$aSingapore :$$bSpringer,$$c[2019] 000890368 264_4 $$c©2019 000890368 300__ $$a1 online resource. 000890368 336__ $$atext$$btxt$$2rdacontent 000890368 337__ $$acomputer$$bc$$2rdamedia 000890368 338__ $$aonline resource$$bcr$$2rdacarrier 000890368 4901_ $$aLecture notes in chemistry ;$$vVolume 103 000890368 504__ $$aIncludes bibliographical references and index. 000890368 5050_ $$aIntro; Preface; Contents; 1 Solid-State NMR Principles and Techniques; 1.1 Introduction; 1.2 Nuclear Spin Interactions in Solids; 1.2.1 Chemical Shift Interaction; 1.2.2 Dipole-Dipole Interaction; 1.2.3 Quadrupolar Interaction; 1.2.4 Spin-Spin Interaction; 1.3 Manipulations of Spin Interactions in Solids; 1.3.1 Magic-Angle Spinning (MAS); 1.3.2 Cross-Polarization; 1.3.3 Dipolar Decoupling Methods in Rotating Solid; 1.3.4 Dipolar Recoupling Methods in Rotating Solid; 1.3.5 High-Resolution Techniques for Half-Integer-Spin Quadrupolar Nuclei; 1.3.6 Summary; References 000890368 5058_ $$a2 Solid-State NMR Studies of Zeolites and Zeotype Materials Synthesis2.1 Introduction; 2.2 Zeolite Synthesis Route and Procedures; 2.3 Zeolite Synthesis Process and Crystallization Mechanism; 2.4 NMR Strategy in Characterization of Zeolite Synthesis; 2.4.1 Microporous Aluminosilicates; 2.4.2 Microporous Aluminophosphates; 2.5 Summary; References; 3 Solid-State NMR Characterization of Framework Structure of Zeolites and Zeotype Materials; 3.1 Introduction; 3.2 Solid-State NMR Characterization of Zeolite Framework Structure; 3.2.1 27Al MAS NMR; 3.2.2 29Si MAS NMR; 3.2.3 31P MAS NMR 000890368 5058_ $$a3.2.4 17O MAS NMR3.2.5 129Xe NMR; 3.2.6 Other Framework Elements; 3.3 Summary; References; 4 Solid-State NMR Characterization of Host-Guest Interactions; 4.1 Introduction; 4.2 Solid-State NMR Characterization of Host-Guest Interactions; 4.2.1 Host-Guest Interaction Between Adsorbed Molecule and Zeolite Framework; 4.2.2 Host-Guest Interaction in Molecular Sieve Synthesis; 4.2.3 Host-Guest Interaction in Zeolite Catalysis; 4.3 Summary; References; 5 Solid-State NMR Characterization of Acid Properties of Zeolites and Solid Acid Catalysts; 5.1 Introduction 000890368 5058_ $$a5.2 Solid-State NMR Characterization of Acidic Property5.2.1 Acid Sites Containing Hydroxyl Groups; 5.2.2 Acidic Nature and Strength; 5.2.3 Location and Distribution of Acid Sites; 5.2.4 Spatial Proximities and Synergy Effects of Different Acid Sites; 5.3 Summary; References; 6 In Situ Solid-State NMR Investigation of Catalytic Reactions on Zeolites; 6.1 Introduction; 6.2 In Situ Solid-State NMR Approaches; 6.2.1 Batch Reaction; 6.2.2 Flow Reaction; 6.3 Mechanistic Study of the Catalytic Reactions by In Situ NMR; 6.3.1 Activation and Conversion of Light Alkanes 000890368 5058_ $$a6.3.2 Methanol-to-Olefins (MTO) Conversion6.4 Summary; References; Index 000890368 506__ $$aAccess limited to authorized users. 000890368 520__ $$aSolid-State NMR Characterization of Heterogeneous Catalysts and Catalytic Reactions provides a comprehensive account of state-of-the-art solid-state NMR techniques and the application of these techniques in heterogeneous catalysts and related catalytic reactions. It includes an introduction to the basic theory of solid-state NMR and various frequently used techniques. Special emphasis is placed on characterizing the framework and pore structure, active site, guest-host interaction, and synthesis mechanisms of heterogeneous catalysts using multinuclear one- and two-dimensional solid-sate NMR spectroscopy. Additionally, various in-situ solid-state NMR techniques and their applications in investigation of the mechanism of industrially important catalytic reactions are also discussed. Both the fundamentals and the latest research results are covered, making the book suitable as a reference guide for both experienced researchers in and newcomers to this field. Feng Deng is a Professor at Wuhan Institute of Physics and Mathematics, Chinese Academy of Sciences. 000890368 588__ $$aVendor-supplied metadata. 000890368 650_0 $$aZeolite catalysts. 000890368 650_0 $$aNuclear magnetic resonance spectroscopy. 000890368 7001_ $$aWang, Qiang,$$eauthor. 000890368 7001_ $$aLi, Shenhui,$$eauthor. 000890368 7001_ $$aDeng, Feng,$$eauthor. 000890368 830_0 $$aLecture notes in chemistry ;$$v103. 000890368 852__ $$bebk 000890368 85640 $$3SpringerLink$$uhttps://univsouthin.idm.oclc.org/login?url=http://link.springer.com/10.1007/978-981-13-6967-4$$zOnline Access$$91397441.1 000890368 909CO $$ooai:library.usi.edu:890368$$pGLOBAL_SET 000890368 980__ $$aEBOOK 000890368 980__ $$aBIB 000890368 982__ $$aEbook 000890368 983__ $$aOnline 000890368 994__ $$a92$$bISE